Scientists are increasingly specializing in narrower fields, and communication is often difficult between physicists researching elementary particles and those studying semiconductors, not to mention between physicists and biologists or doctors. This makes interdisciplinary work difficult. And yet sometimes they succeed. One thread of work underway at the PAS Institute of High Pressure Physics offers a good example.
The high-pressure torsion (HPT) of Ti-Fe alloys with different iron content has been studied at 7 GPa, 5 anvil rotations and rotation speed of 1 rpm. The alloys have been annealed before HPT in such a way that they contained different amounts of α/α' and β phases. In turn, the β phase contained different concentration of iron. The 5 anvil rotations correspond to the HPT steady-state and to the dynamic equilibrium between formation and annihilation of microstructure defects. HPT leads to the transformation of initial α/α' and β-phases into mixture of α and high-pressure ω-phase. The α → ω and β → ω phase transformations are martensitic, and certain orientation relationships exist between α and ω as well as β and ω phases. However, the composition of ω-phase is the same in all samples after HPT and does not depend on the composition of β-phase (which is different in different initial samples). Therefore, the martensitic (diffusionless) transformations are combined with a certain HPT-driven mass-transfer. We observed also that the structure and properties of phases (namely, α-Ti and ω-Ti) in the Ti – 2.2 wt. % Fe and Ti – 4 wt. % Fe alloys after HPT are equifinal and do not depend on the structure and properties of initial α'-Ti and β-Ti before HPT.
The article concerns investigations over benefits of application of HRC devices into sulphide copper ore processing plant. High pressure comminution appears to be very effective technology in hard ore processing circuits, especially in terms of energy consumption. This can be particularly observed in downstream grinding and beneficiation operations. A series of pilot-scale crushing tests in HRC roller press for various levels of operating pressure, were performed. HRC crushing effectiveness along with downstream grinding process course for each crushing product were also under analysis. The investigations were supplemented by analysis of flotation process effectiveness and impact of the process of high-pressure comminution on environment (dust emission). The results of investigation show that operating pressure level influences the obtained comminution results (comminution degree, yield of finest particle size fractions). The grinding effectiveness, measured through production of the finest particle size fractions was significantly influenced by the operating pressure. The results show that higher values of operating pressure (4.0 and 4.5 N/mm2) are not as efficient within this scope as the pressure 3.5 N/mm2. Dust emission is also correlated with the operating pressure value.
Magnesium alloys are one of the lightest of all the structural materials. Because of their excellent physical and mechanical properties the alloys have been used more and more often in various branches of industry. They are cast mainly (over 90%) on cold and hot chamber die casting machines. One of the byproducts of casting processes is process scrap which amounts to about 40 to 60% of the total weight of a casting. The process scrap incorporates all the elements of gating systems and fault castings. Proper management of the process scrap is one of the necessities in term of economic and environmental aspects. Most foundries use the process scrap, which involves adding it to a melting furnace, in a haphazard way, without any control of its content in the melt. It can lead to many disadvantageous effects, e.g. the formation of a hard buildup at the bottom of the crucible, which in time makes casting impossible due to the loss of the alloy rheological properties. The research was undertaken to determine the effect of an addition of the process scrap on the mechanical properties of AZ91 and AM50 alloys. It has been ascertained that the addition of a specific amount of process scrap to the melt increases the mechanical properties of the elements cast from AZ91 and AM50 alloys. The increase in the mechanical properties is caused mainly by compounds which can work as nuclei of crystallization and are introduced into the scrap from lubricants and anti-adhesive agents. Furthermore carbon, which was detected in the process scrap by means of SEM examination, is a potent grain modifier in Mg alloys [1-3]. The optimal addition of the process scrap to the melt was determined based on the statistical analysis of the results of studies of the effect of different process scrap additions on the mean grain size and mechanical properties of the cast parts.
Experimental Mg-Al-RE type magnesium alloys for high-pressure die-casting are presented. Alloys based on the commercial AM50 magnesium alloy with 1, 3 and 5 mass % of rare earth elements were fabricated in a foundry and cast in cold chamber die-casting machines. The obtained experimental casts have good quality surfaces and microstructure consisting of an α(Mg)-phase, Al11RE3, Al10RE2Mn7 intermetallic compound and small amount of α+γ eutectic and Al2RE phases.
The paper deals with experimental investigations of a set of metal "2-delta" gaskets of different depth. The gaskets were examined under assembly conditions, i.e. placed in their seats and loaded with the compressive assembly force with no operating pressure applied to the closure. The electric resistance wire strain gauges were used to measure the circumferential and axial strains at the inner cylindrical surface of the gaskets. The plastic deformations of the contact surface of the seats were measured after disassembly of the closures. The material tests were carried out to determine real mechanical properties of materials applied for the gaskets and the seats. The results of experiment were compared with the analytical approach. The plastic deformations were taken into account in the analytical solution of the contact region between the gasket and the seats. The results of experiment and analytical approach were verified by FEM calculations, which take into account linear hardening of the material, friction and contact effects.
The nonlinearity parameter B/A, internal pressure, and acoustic impedance are calculated for a room temperature ionic liquid, i.e. for 1-ethyl-3-methylimidazolium bis[(trifluoromethyl)sulfonyl]imide for temperatures from (288.15 to 318.15) K and pressures up to 100 MPa. The B/A calculations are made by means of a thermodynamic method. The decrease of B/A values with the increasing pressure is observed. At the same time B/A is temperature independent in the range studied. The results are compared with corresponding data for organic molecular liquids. The isotherms of internal pressure cross at pressure in the vicinity of 70 MPa, i.e. in this range the internal pressure is temperature independent.
The paper presents the results of investigations concerning the influence of negative (relative) pressure in the die cavity of high pressure die casting machine on the porosity of castings made of AlSi9Cu3 alloy. Examinations were carried out for the VertaCast cold chamber vertical pressure die casting machine equipped with a vacuum system. Experiments were performed for three values of the applied gauge pressure: -0.3 bar, -0.5 bar, and -0.7 bar, at constant values of other technological parameters, selected during the formerly carried initial experiments. Porosity of castings was assessed on the basis of microstructure observation and the density measurements performed by the method of hydrostatic weighing. The performed investigation allowed to find out that – for the examined pressure range – the porosity of castings decreases linearly with an increase in the absolute value of negative pressure applied to the die cavity. The negative pressure value of -0.7 bar allows to produce castings exhibiting porosity value less than 1%. Large blowholes arisen probably by occlusion of gaseous phase during the injection of metal into the die cavity, were found in castings produced at the negative pressure value of -0.3 bar. These blowholes are placed mostly in regions of local thermal centres and often accompanied by the discontinuities in the form of interdendritic shrinkage micro-porosity. It was concluded that the high quality AlSi9Cu3 alloy castings able to work in elevated temperatures can be achieved for the absolute value of the negative pressure applied to the die cavity greater than 0.5 bar at the applied set of other parameters of pressure die casting machine work.
The presented work is aimed to deal with the influence of changes in the value of negative (relative) pressure maintained in the die cavity of pressure die casting machine on the surface quality of pressure castings. The examinations were held by means of the modified Vertacast pressure die casting machine equipped with a vacuum system. Castings were produced for the parameters selected on the basis of previous experiments, i.e. for the plunger velocity in the second stage of injection at the level of 4 m/s, the pouring temperature of the alloy equal to 640°C, and the die temperature of 150°C. The examinations were carried on for three selected values of negative gauge pressure: - 0.03, - 0.05, and - 0.07 MPa. The quality of casting was evaluated by comparing the results of the surface roughness measurements performed for randomly selected castings. The surface roughness was measured by means of Hommel Tester T1000. After a series of measurements it was found that the smoothest surface is exhibited by castings produced at negative gauge pressure value of - 0.07 MPa.
The present contribution reports on the rheological investigations concerning influence of high hydrostatic pressure on the molecular structure of gelatin gels. For the purpose of the study, a torsional shear wave rheometer for in-situ investigations of viscoelastic substances under high pressure was developed. Small amplitude vibrations generated by piezoelectric elements are used to determine the storage modulus of the investigated medium. The system is able to stand pressures up to 300 MPa. The experiments have been carried out with household gelatin (0.1 w/w aqueous solution). The gelification curves revealed similar time course. However, the values of G0 obtained for the gels curing 300 minutes under 100 MPa and 200 MPa were observed to be respectively 2.1 and 4 times higher than at ambient conditions. The increased number of triple helix junction zones is hypothesised to be the cause of this phenomenon as a result of reinforcement of the hydrogen bonds due to pressure. An attempt to cognize the characteristic dimensions of the molecular structure based on the theory of rubber elasticity is made.
The present work discusses results of increased temperature on shape-dimensional changes of a 110 type hose coupling, produced from EN AC-AlSi11 alloy with the use of pressure die casting technology. The castings were soaked for 3.5 h at temperatures 460°C, 475°C and 490°C. The verification of shape-dimensional accuracy of the elements after soaking treatment, in relation to raw casting, was carried out by comparing the 3D models received from 3D scanning. Soaking temperature of about 460°C-475°C results in no significant changes in the shapes and dimensions of the castings, or surface defects in the form of blisters, which can be seen at a temperature of 490°C.
Development of salt cores prepared by high-pressure squeezing and shooting with inorganic binders has shown a high potential of the given technology even for high-pressure casting of castings. Strength, surface quality of achieved castings, and solubility in water become a decisive criterion. The shape and quality of grain surface particularly of NaCl – cooking salts that can be well applied without anticaking additives has shown to be an important criterion. Thus the salt cores technology can cover increasingly growing demands for casting complexity especially for the automobile industry.
The poorly cemented Ciężkowice poorly sorted sandstone and the compact Mucharz fine grain sandstone have been laboratory tested at the triaxial compressing conditions in thermo-pressurized chamber of a rigid press MTS-815. The confining pressure: P = σ₂ = gσ₃ range from 0 to 96 MPa and the temperature: T from 22°C to 120°C (simulated 500 m intervals from the surface to the depth of 3500 m). During (the) each test, the characteristics of deformation and the elastic wave velocity paths were simultaneously monitored. The volume density and longitudinal wave velocity showed a non-linear increase with the progress of simulated depth, a volume density growth by 1.6 to 4.0%, and the elastic wave velocity up to 250% of the primary value (surface condition), dependable on loading path, phase of deformation, and varying type of lithology. That may lead to wide error margin in a determination of rock’s engineering properties and also create discrepancies between the static parameters of rocks (Est, gνst) determined by standard laboratory load tests, and the dynamic parameters (Ed, νd) determined from the wave velocity and volume density.
The paper deals with experimental investigations of a set of metal wave-ring gaskets of different thickness and different assembly interference. The gaskets were examined under assembly conditions, i.e. pressed in their seats with no operating pressure applied. The electric resistance wire strain gauges were used to measure the circumferential and axial strains at the inner surface of the gaskets. The traces of contact at the working surface of the gaskets were measured after disassembly the gaskets from their seats. The material tests were carried out to determine the real mechanical properties of materials applied for the gaskets and the seats. The results of experiment were verified by FEM calculations and compared with the analytical approach based on the simplified shell model proposed for the gasket.
A measuring system was developed for the measurement of ejector forces in the die casting process. When selecting the sensor technology, particular care was taken to ensure that measurements can be taken with a high sampling rate so that the fast-running ejection process can be recorded. For this reason, the system uses piezoelectric force sensors which measure the forces directly at the individual ejector pins. In this way, depending on the number of sensors, it is possible to determine both the individual ejector forces and the total ejector force. The system is expandable and adaptable with regard to the number and position of the sensors and can also be applied to real HPDC components. Automatic triggering of the measurements is also possible. In addition to the measuring system, a device and a method for in-situ calibration of the sensors have also been developed. To test the measuring system, casting experiments were carried out with a real aluminium HPDC aluminium component. The experiments showed that it is possible to measure the ejector forces with sufficient sampling rate and also to observe the process steps of filling, intensification and die opening by means of ejector forces. Experimental setup serves as a basis for future investigations regarding the influencing parameters on the ejection process.
The paper deals with problem of optimal used automatic workplace for HPDC technology - mainly from aspects of operations sequence, efficiency of work cycle and planning of using and servicing of HPDC casting machine. Presented are possible ways to analyse automatic units for HPDC. The experimental part was focused on the rationalization of the current work cycle time for die casting of aluminium alloy. The working place was described in detail in the project. The measurements were carried out in detail with the help of charts and graphs mapped cycle of casting workplace. Other parameters and settings have been identified. The proposals for improvements were made after the first measurements and these improvements were subsequently verified. The main actions were mainly software modifications of casting center. It is for the reason that today's sophisticated workplaces have the option of a relatively wide range of modifications without any physical harm to machines themselves. It is possible to change settings or unlock some unsatisfactory parameters.
The paper concerns the problem of discontinuity in high pressure die castings (HPDC). The compactness of their structure is not perfect, as it is sometimes believed. The discontinuities present in these castings are the porosity as follow: shrinkage and gas (hydrogen and gas-air occlusions) origin. The mixed gas and shrinkage nature of porosity makes it difficult to identify and indicate the dominant source. The selected parameters of metallurgical quality of AlSi9Cu3 alloy before and after refining and the gravity castings samples (as DI - density index method), were tested and evaluated. This alloy was served to cast the test casting by HPDC method. The penetrating testing (PT) and metallographic study of both kinds of castings were realized. The application of the NF&S simulation system allowed virtually to indicate the porosity zones at risk of a particular type in gravity and high-pressure-die-castings. The comparing of these results with the experiment allowed to conclude about NF&S models validation. The validity of hypotheses concerning the mechanisms of formation and development of porosity in HPDC casting were also analyzed.
The impact of casting conditions on microstructure a and mechanical properties was described, especially for cast products from AlSi9Cu3 alloy. Particular attention was paid to the parameters of dendritic structure: DAS 1 and DAS 2. Selected mechanical properties (by static tension test) of test castings made using basic technologies of casting: GSC - gravity sand casting, GDC - gravity die-casting and HPDC - high-pressure die-casting, are presented for cast-on test bars and cast separately. Casts were made of the same alloy AlSi9Cu3. Fractures and the zone near the fracture (after static tension test) was subjected to VT - visual tests, PT - penetration tests and metallographic tests. The condition of porosity (fracture zone) was also assessed. The analysis of virtual results was performed using the NovaFlow & Solid system together with the database and they were compared to experimental tests. This way of validation was applied in order to assess the correlation between the local rate of cooling and the size of DAS for GSC, GDC and HPDC technologies. Finally, the correlation between the parameters of structure and mechanical properties with regard to the impact of porosity was signalized.