This paper discusses the influence of the direction of applied deformation on the ability to gelation of thermosensitive chitosan hydrogels. The application of the shear rate equal in value to the classically performed oscillatory measurements leads to significantly different shapes of experimental curves. It was found that the type of mechanically applied deformation has a significant impact on the gelation ability of colloidal chitosan solutions and conditions of sol-gel phase transition. Simple shear leads to a phase transition at a lower temperature or in a shorter time compared to oscillatory tests. Moreover, based on the final values of dynamic viscosity in rotational measurements, it was found that stronger crosslinking of the polymer structure was observed.
An optical tomograph in which a tested object is illuminated from five directions has been presented in the paper. The measurements of luminous intensity after changing into discrete signals (0 or 1) in the detectors equipped with 64 optical sensors were subjected to reconstruction by means of the matrix algorithm. Detailed description of the measuring sensor, as well as the principles of operation of the electronic system, has been given in the paper. Optical phenomena occurring at the phase boundary while transmitted through the sensor wall and phenomena inside the measuring space have also been taken into account. The method of the sensor calibration has been analysed and a way of technical solution of the problem under consideration has been discussed. The elaborated method has been tested using objects of the known shape and dimensions. It was found that reconstruction of the shapes of moving bubbles and determination of their main parameters is also possible with a reasonable accuracy.
The present work offers new equations for phase evaluation in measurements. Several phase-shifting equations with an arbitrary but constant phase-shift between captured intensity signs are proposed. The equations are similarly derived as the so called Carré equation. The idea is to develop a generalization of the Carré equation that is not restricted to four images. Errors and random noise in the images cannot be eliminated, but the uncertainty due to their effects can be reduced by increasing the number of observations. An experimental analysis of the errors of the technique was made, as well as a detailed analysis of errors of the measurement. The advantages of the proposed equation are its precision in the measures taken, speed of processing and the immunity to noise in signs and images.
Passive radar does not have its own emitter. It uses so-called signals of opportunity emitted by non-cooperative illuminators. During the detection of reflected signals, a direct signal from a non-cooperative emitter is used as the reference signal. Detection of electromagnetic echoes is, in present day radars, performed by finding the maximum of the cross ambiguity function. This function is based on the multiplication of the received signal and the reference signal. Detection of echoes by means of a quadrature microwave phase discriminator QMPD was proposed in the work as an alternative solution for ambiguity function evaluation. This discriminator carries out vectorial summing of the received and the reference signals. The summing operations in QMPD are carried out with the aid of microwave elements and without the use of expensive digital signal processors. Definitions of the phase and phase difference of the so-called simple signals and noise signals were described. A proposal of a passive radar equipped with several independent quadrature microwave phase discriminators was presented. Ideas of algorithms of object detection and of the distance-to-object estimation designed for this radar have been also sketched.
The phase jitter enables to assess quality of signals transmitted in a bi-directional, long-distance fibre optic link dedicated for dissemination of the time and frequency signals. In the paper, we are considering measurements of jitter using a phase detector the detected frequency signal and the reference signal are supplied to. To cover the wideband jitter spectrum the detected signal frequency is divided and – because of the aliasing process – higher spectral components are shifted down. We are also examining the influence of a residual jitter that occurs in the reference signal generated by filtering the jitter occurring in the same signal, whose phase fluctuations we intend to measure. Then, we are discussing the evaluation results, which were obtained by using the target fibre optic time and frequency transfer system.
Determination of the phase difference between two sinusoidal signals with noise components using samples of these signals is of interest in many measurement systems. The samples of signals are processed by one of many algorithms, such as 7PSF, UQDE and MSAL, to determine the phase difference. The phase difference result must be accompanied with estimation of the measurement uncertainty. The following issues are covered in this paper: the MSAL algorithm background, the ways of treating the bias influence on the phase difference result, comparison of results obtained by applying MSAL and the other mentioned algorithms to the same real signal samples, and evaluation of the uncertainty of the phase difference.
Most systems used in quantum physics experiments require the efficient and simultaneous recording different multi-photon coincidence detection events. In such experiments, the single-photon gated counting systems can be applicable. The main sources of errors in these systems are both instability of the clock source and their imperfect synchronization with the excitation source. Below, we propose a solution for improvement of the metrological parameters of such measuring systems. Thus, we designed a novel integrated circuit dedicated to registration of signals from a photon number resolving detectors including a phase synchronizer module. This paper presents the architecture of a high-resolution (~60 ps) digital phase synchronizer module cooperating with a multi-channel coincidence counter. The main characteristic feature of the presented system is its ability to fast synchronization (requiring only one clock period) with the measuring process. Therefore, it is designed to work with various excitation sources of a very wide frequency range. Implementation of the phase synchronizer module in an FPGA device enabled to reduce the synchronization error value from 2.857 ns to 214.8 ps.