In this paper is discussed the effect of the inoculant mischmetal addition on the microstructure of the magnesium alloy AZ91. The concentration of the inoculant was increased in the samples within the range from 0.1% up to 0.6%. The thermal process was performed with the use of Derivative and Thermal Analysis (DTA). A particular attention was paid to finding the optimal amount of the inoculant, which causes fragmentation of the microstructure. The concentration of each element was verified with use of a spark spectrometer. In addition, the microstructures of every samples were examined with the use of an optical microscope and also was performed an image analysis with a statistical analysis using the NIS–Elements program. The point of those analyses was to examine the differences in the grain diameters of phase αMg and eutectic αMg+γ(Mg17Al12) in the prepared samples as well as the average size of each type of grain by way of measuring their perimeters. This paper is the second part of the introduction into a bigger research on grain refinement of magnesium alloys, especially AZ91. Another purpose of this research is to achieve better microstructure fragmentation of magnesium alloys without the relevant changes of the chemical composition, which should improve the mechanical properties.
The work presents results of the investigations of effect of intensive cooling of alloy AC-AlSi7Mg with alloy additions on microstructure and mechanical properties of the obtained casts. The experimental casts were made in ceramic molds preliminarily heated to 180°C, into which AC-AlSi7Mg with alloy additions was poured. Within implementation of the research, a comparison was made of the microstructure and mechanical properties of the casts obtained in ceramic molds cooled at ambient temperature and the ones intensively cooled in a cooling liquid. Kinetics and dynamics thermal effects recorded by the TDA method were compared. Metallographic tests were performed with the use of optical microscope and strength properties of the obtained casts were examined: UTS, Elongation and HB hardness.
The study presents the results of the investigations of the effect of Cu, Ni, Cr, V, Mo and W alloy additions on the microstructure and mechanical properties of the AlSi7Mg0.3 alloy. The examinations were performed within a project the aim of which is to elaborate an experimental and industrial technology of producing elements of machines and devices complex in their construction, made of aluminium alloys by the method of precision investment casting. It was demonstrated that a proper combination of alloy additions causes the crystallization of complex intermetallic phases in the silumin, shortens the SDAS and improves the strength properties: Rm, Rp0.2,HB hardness. Elevating these properties reduces At, which, in consequence, lowers the quality index Q of the alloy of the obtained casts. Experimental casts were made in ceramic moulds preliminarily heated to 160 °C, into which the AlSi7Mg0.3 alloy with the additions was cast, followed by its cooling at ambient temperature. With the purpose of increasing the value of the quality index Q, it is recommended that the process of alloy cooling in the ceramic mould be intensified and/or a thermal treatment of the casts be performed (ageing)(T6).
The work presents the test result of the influence of cooling rate on the microstructure of AZ91 alloy, Vickers micro-hardness and Brinell hardness. Studies cooling and crystallization of AZ91 alloy was cast into the ceramic shells pre-heated to 180 ° C and then air-cooled at ambient temperature or intensively super cooled in the liquid coolant. The TDA method was applied to record and characterize the thermal effect resulting from the phase transformations occurring during the crystallization of AZ91 alloy. The kinetics and dynamics of the thermal processes of crystallization of AZ91 alloy in the ceramic shells were determined. Metallographic tests were performed with the use of an optical microscope. A comparison of these test results with the thermal effect recorded by way of the TDA method was made. Influence of cooling rate of AZ91 on HV0, 01 micro-hardness and Brinell hardness alloy was examined.
The work presents the results of the investigations of the effect of inhibitors coated on the internal walls of a ceramic mould on the quality of the obtained casts made of the AM60 alloy containing additions of chromium and vanadium. In order to reduce the reactivity of magnesium alloy cast by the technology of investment casting with the material of the mould and the ambient atmosphere, solid inhibitors were applied in the form of a mixture of KBF4 and H3BO3 after the stage of mould baking and before the mould’s being filled with the liquid alloy. For the purpose of examining the effect of the inhibitors on the surface quality of the obtained casts, profilometric tests were performed and the basic parameters describing the surface roughness, Ra, Rz and Rm, were determined.